SPME of Polyphenols in Wine and Grapes
Researchers from the University of Murcia (Murcia, Spain) developed a sample pretreatment system based on solid-phase microextraction (SPME) followed by gas chromatography with mass spectrometry detection (GC?MS).
Researchers from the University of Murcia (Murcia, Spain) developed a sample pretreatment system based on solid-phase microextraction (SPME) followed by gas chromatography with mass spectrometry detection (GC–MS). They used a direct immersion SPME technique to adsorb the polyphenols and then placed the SPME fiber into the headspace of a BSTFA solution for derivatization for 15 min at 50 °C. They desorbed the analytes at 280 °C for 5 min. They were able to determine the analytes cis- and trans-resveratrol, piceatannol, catechin, and epicatechin in wine and grapes.
Analytical Challenges in Measuring Migration from Food Contact Materials
November 2nd 2015Food contact materials contain low molecular weight additives and processing aids which can migrate into foods leading to trace levels of contamination. Food safety is ensured through regulations, comprising compositional controls and migration limits, which present a significant analytical challenge to the food industry to ensure compliance and demonstrate due diligence. Of the various analytical approaches, LC-MS/MS has proved to be an essential tool in monitoring migration of target compounds into foods, and more sophisticated approaches such as LC-high resolution MS (Orbitrap) are being increasingly used for untargeted analysis to monitor non-intentionally added substances. This podcast will provide an overview to this area, illustrated with various applications showing current approaches being employed.
AI-Powered Precision for Functional Component Testing in Tea Analysis
October 11th 2024Analyzing functional foods reveals numerous health benefits. These foods are rich in bioactive compounds that go beyond basic nutrition, boosting the immune system and improving overall wellness. However, analyzing these compounds can be challenging. This article discusses AI algorithms to support automated method development for liquid chromatography, simplifying the process, enhancing labor efficiency, and ensuring precise results, making it accessible to non-experts for tea analysis.
Advanced LC–MS Analysis for PFAS Analysis in Eggs
October 11th 2024The European Commission's regulation on maximum levels for certain contaminants in food highlights the need for precise and reliable methods to quantify per- and polyfluoroalkyl substances (PFAS) in various food matrices. This article discusses development and validation of a robust method for analyzing 21 PFAS compounds in chicken eggs using solid-phase extraction (SPE) and liquid chromatography–mass spectrometry (LC–MS).
