|Articles|February 1, 2004

LCGC North America

  • LCGC North America-02-01-2004
  • Volume 22
  • Issue 2

Developments in 2-D Gas Chromatography with Heartcutting

This review discusses the operating principles of and current applications for two-dimensional gas chromatography with heartcutting.


Related to this article

Figure 2. Split injection used to measure triplicate test of MTBE, hexane, o-xylene, and 1-methylnaphthalene comparing different solvents (methanol, methylene chloride) and column insertion distances starting with 0.5 mm, 5.0 mm, 10.0 mm, 15 mm, and 20.0 mm. Methanol had the best performance at the 5.0 mm insertion distance and methylene chloride looked slightly better at the 0.5 mm. We would still recommend not going below the 5.0 mm manufacturer recommended insertion distance.
Revisiting insertion distance for methanol and methylene chloride in GC analysis and confirming that insertion depth strongly affects response and reproducibility.