|Articles|May 1, 2008

LCGC North America

  • LCGC North America-05-01-2008
  • Volume 26
  • Issue 5

Peaks of Interest-Scientists Develop Method for Identifying Gunshot Residue

Scientists Jorn Chi Chung Yu, Garrett Lee Burleson, and colleagues in the Department of Forensic Science at Sam Houston State University in Texas have developed a new method for identifying gunshot residue without the presence of lead.

Scientists Jorn Chi Chung Yu, Garrett Lee Burleson, and colleagues in the Department of Forensic Science at Sam Houston State University in Texas have developed a new method for identifying gunshot residue without the presence of lead.

Due to environmental and health concerns surrounding the use of lead, "lead-free" ammunition has become more popular, which presents a problem for forensic scientists that rely on lead-based residue tests. The new technique utilizes the analysis of gas chromatography data coupled with results from a nitrogen phosphorus detector, requires just a tiny speck of residue, and uses no extraction reagents.

"The main focus of our research is to develop a method that will help credibility of gunshot residue evidence in court. You can get results in 30 to 40 minutes with the new test. In addition you only need small amounts of evidence to run the test," Burleson said.


Related to this article

Figure 2. Split injection used to measure triplicate test of MTBE, hexane, o-xylene, and 1-methylnaphthalene comparing different solvents (methanol, methylene chloride) and column insertion distances starting with 0.5 mm, 5.0 mm, 10.0 mm, 15 mm, and 20.0 mm. Methanol had the best performance at the 5.0 mm insertion distance and methylene chloride looked slightly better at the 0.5 mm. We would still recommend not going below the 5.0 mm manufacturer recommended insertion distance.
Revisiting insertion distance for methanol and methylene chloride in GC analysis and confirming that insertion depth strongly affects response and reproducibility.
Sam Whitmarsh, Nitish Sharma, Piotr Alvarez, GLP-1 Peer Exchange
Meet the expert panel exploring the challenges involved in GLP-1 analysis in this LCGC International Peer Exchange®.
Chromatography Detects Toxins in Tea Samples
High-performance liquid chromatography-tandem mass spectroscopy (HPLC–MS/MS) chromatography reveals pyrrolizidine alkaloids (PA)/pyrrolizidine alkaloid N-oxides (PANO) toxin risks in 63 tea samples.