|Articles|June 30, 2004

LCGC North America

  • LCGC North America-07-01-2004
  • Volume 22
  • Issue 7

The Retention Gap Effect

The effects of adding a precolumn - or retention gap - to a capillary column are explored.

Articles in this issue

about 22 years ago

ChromAuctions

about 22 years ago

July TOC

about 22 years ago

Supplement to GC Connections

about 22 years ago

Peaks of Interest

about 22 years ago

Divide and Conquer

Related to this article

Figure 2. Split injection used to measure triplicate test of MTBE, hexane, o-xylene, and 1-methylnaphthalene comparing different solvents (methanol, methylene chloride) and column insertion distances starting with 0.5 mm, 5.0 mm, 10.0 mm, 15 mm, and 20.0 mm. Methanol had the best performance at the 5.0 mm insertion distance and methylene chloride looked slightly better at the 0.5 mm. We would still recommend not going below the 5.0 mm manufacturer recommended insertion distance.
Revisiting insertion distance for methanol and methylene chloride in GC analysis and confirming that insertion depth strongly affects response and reproducibility.