This article presents SFC and UHPLC—both coupled with HRMS—methods for the analysis of short-, medium-, and long-chain CPs in fish oil-based dietary supplements.
In this study, SFC and UHPLC—both coupled with HRMS—methods for the analysis of short-, medium-, and long-chain CPs in fish oil-based dietary supplements were developed and validated at concentration levels of 0.6 and 3.0 µg/g lipid weight (lw).
The aim of this study was to develop an efficient method to enable a rapid determination of nine 3-MCPDEs and seven GEs in vegetable oils within a single run employing supercritical fluid chromatography coupled to high-resolution tandem mass spectrometry (SFC–HRMS/MS).