Researchers from the Chinese Academy of Sciences (Beijing, China) and the University of Science and Technology of China (Hefei, China) used a two- and three-phase hollow-fiber liquid-phase microextraction method to determine aromatic amines in environmental water samples.
Researchers from the Chinese Academy of Sciences (Beijing, China) and the University of Science and Technology of China (Hefei, China) used a two- and three-phase hollow-fiber liquid-phase microextraction method to determine aromatic amines in environmental water samples. The analytes were aniline, 4-nitroaniline, 2,4-dinitroaniline, and dicloran, and they were extracted from basic aqueous samples into the organic membrane phase of the hollow fiber’s wall and then were back extracted into an acidified aqueous acceptor solution in the lumen of the fiber. According to the researchers, the method worked well with real environmental water samples with microgram per liter level analytes.
HPLC 2025 Preview: Functionalized Monoliths as Selective Sample Preparation Materials
May 16th 2025Analyzing trace compounds from complex samples often requires purification and pre-concentration, and online coupling of solid-phase extraction (SPE) with liquid chromatography (LC) helps minimize analysis time and solvent/sample use. Monoliths with large macropores are ideal for this coupling due to their low back pressure and versatility in various formats.
Thermodynamic Insights into Organic Solvent Extraction for Chemical Analysis of Medical Devices
April 16th 2025A new study, published by a researcher from Chemical Characterization Solutions in Minnesota, explored a new approach for sample preparation for the chemical characterization of medical devices.