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An Improved Analytical Temperature-Rising Elution Fractionation System for Automated Analysis of Polyethylenes
Alain M. Jonas
Catholic University of Louvain, Unite de Physique et de Chimie des Hauts Polymeres, Batiment Boltzmann, Place Croix du Sud, 1, B-1348 Louvain-la-Neuve, Belgium.
Adrian G. Boborodea
Catholic University of Louvain, Unite de Physique et de Chimie des Hauts Polymeres, Batiment Boltzmann, Place Croix du Sud, 1, B-1348 Louvain-la-Neuve, Belgium and Polytechnical University of Bucharest, department of Polymer Physics, 149 Calea Victoriei, Sector 1, bucharest, Romania.
Daniel Daoust
Catholic University of Louvain, Unite de Physique et de Chimie des Hauts Polymeres, Batiment Boltzmann, Place Croix du Sud, 1, B-1348 Louvain-la-Neuve, Belgium.
Christian Bailly
Catholic University of Louvain, Unite de Physique et de Chimie des Hauts Polymeres, Batiment Boltzmann, Place Croix du Sud, 1, B-1348 Louvain-la-Neuve, Belgium.
LCGC North America
The authors describe a system for automated analytical temperature-rising elution fractionation that uses the built-in differential refractometer of a commercial gel-permeation chromatography instrument and a stop-flow method for sample crystallization.