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LCGC Europe-06-01-2013
LCGC Europe
Determination of Phytohormones in Plant Extracts Using In-matrix Ethyl Chloroformate Derivatization and DLLME–GC–MS
June 01, 2013
Cover Story
26
6
A fast and simple sample preparation method for the simultaneous determination of 11 phytohormones in plants by GC–MS has been developed.
Gradient Elution, Part IV: Dwell-Volume Problems
June 01, 2013
LC Troubleshooting
26
6
Gradient methods can offer unique solutions to separations problems, but transferring a gradient method from the literature, between laboratories, or even within the same laboratory can be a challenging process.
Hydrogen Deuterium Exchange Mass Spectrometry: An Emerging Biophysical Tool for Probing Protein Behaviour and Higher-Order Structure
June 01, 2013
MS–The Practical Art
26
6
This article looks at how hydrogen-deuterium exchange mass spectrometry (HDX-MS), an MS-based labelling approach, has begun to serve as a means for performing routine biophysical analysis.
Simple and Fast Quantification of Capsaicinoids in Hot Sauces Using Monolithic Silica Capillaries and LC–MS
June 01, 2013
Feature
26
6
The authors describe a simple and fast quantification method to determine capsaicinoids in hot sauces extracted from a wide range of sources, including hot sauces and sausages.
Troubleshooting GC Retention-Time, Efficiency, and Peak-Shape Issues
June 01, 2013
The Essentials
26
6
Problems with the chromatogram can often reveal underlying problems with methods or instrumentation and learning to recognize and fix these problems is essential for all chromatographers.
How Complete Are Your Chromatographic Data?
June 01, 2013
Questions of Quality
26
6
This article will explore what is meant by "complete data" in the context of a chromatography data system and, with an analysis of FDA 483 citations, explore the problems when a laboratory fails to understand this phrase.
Vol 26 No 6 LCGC Europe June 2013 Regular Issue PDF
June 01, 2013
Issue PDF
26
6
Click the title above to open the LCGC Europe June 2013 regular issue, Vol 26 No 6, in an interactive PDF format.