This application news presents instrument operating conditions and
instrument method performance statistics, including method linearity, accuracy, and precision,
for priority pollutant pesticides and PCB congeners. The method validated in this application acted
as guidance in developing ASTM D8543 Test Method for Determination of OCPs and PCBs in
Aqueous Solution by a GC/MS/MS which is intended for proposal to EPA as an alternative test
procedure (ATP) for EPA 608.3
Ultrahigh-performance liquid chromatography–tandem mass spectrometry (UHPLC–MS/MS) tracks blood metabolite changes after repetitive transcranial magnetic stimulation (rTMS)-cognitive training therapy.
Revisiting insertion distance for methanol and methylene chloride in GC analysis and confirming that insertion depth strongly affects response and reproducibility.
A novel SFC–QTOF-MS method accurately detected 10 drugs in oral fluid, matching LC–MS/MS in 83 DUID cases while reducing run time by 42% and organic solvent use by 81%.
Supercritical fluid extraction (SFE) and high-pressure liquid chromatography (HPLC) team up to recover olive waste antioxidants. Marina Russo of the University of Messina (Italy) discusses the details.
Waters' Erin Chambers says combining column chemistry and particle-physics innovation cut a GLP-1 impurity profiling workflow from three hours to under one.