|Articles|September 1, 2001

LCGC North America

  • LCGC North America-09-01-2001
  • Volume 19
  • Issue 9

Gas Chromatography at the 24th International Symposium on Capillary Chromatography and Electrophoresis

In this month's installment, John Hinshaw reports about the 24th International Symposium on Capillary Chromatography and Electrophoresis held in May.


Related to this article

Figure 2. Split injection used to measure triplicate test of MTBE, hexane, o-xylene, and 1-methylnaphthalene comparing different solvents (methanol, methylene chloride) and column insertion distances starting with 0.5 mm, 5.0 mm, 10.0 mm, 15 mm, and 20.0 mm. Methanol had the best performance at the 5.0 mm insertion distance and methylene chloride looked slightly better at the 0.5 mm. We would still recommend not going below the 5.0 mm manufacturer recommended insertion distance.
Revisiting insertion distance for methanol and methylene chloride in GC analysis and confirming that insertion depth strongly affects response and reproducibility.