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An investigation into the Scotch malt whisky brewing practices of over 100 years ago has revealed some unexpected results.

PARKER - CONVERT FROM HE TO H2 AS A CARRIER GAS

A team of researchers has proved that the Ancient Mayans used tobacco. The discovery was prompted by the examination of several ancient Mayan containers from the Kislak Collection of the US Library of Congress for the presence of alkaloids.

LCGC is planning to publish the next issue of The Application Notebook special supplement in June.

How cells survive, replicate and maintain genome integrity in high NaCl concentrations has long puzzled scientists. A group of US scientists has conducted a series of experiments to determine how this occurs and discovered that cells are actually protected from these conditions by the ?gene deserts?, the 40% of the genome that are thought to serve no purpose.

Event news summary

Detection, analysis, and characterization of low-abundant metabolites remain an unresolved problem in metabolic studies. In this study, we report a novel approach to address this challenge. The current methodology is derived from the predictive multiple reaction monitoring (pMRM) mode available on triple-quadrupole linear ion trap mass spectrometry (MS) systems. The pMRM mode offers the highest sensitivity among various acquisition modes for studying trace levels of metabolites of the herbicide clomazone in plants. Additionally, this method allows for the identification of positional isomers of metabolites.

The forging of vehicle registration documents has seen a sharp rise in recent years, with the issue being particularly problematic in Brazil.

In comparison to other GPC/SEC detectors such as light-scattering detectors or UV detectors, viscometers need more care. It takes a longer time to get a stable baseline after changing from one solvent to another and the quality of the LC components plays an important role. Nevertheless, a viscometer is worth these efforts as it provides unique information that is not available with any other detector.

ARABLAB, the annual gathering of the analytical industry in Dubai, is once again recording substantial growth, not only in the Middle East but also throughout the world. With further hall space added for the 2012 event, there are even more opportunities for sellers and buyers to meet and discuss the latest products and services.

Click the title above to open the LCGC North America February 2012 regular issue, Vol 30 No 2, in an interactive PDF format.

Click the title above to open the LCGC North America February 2012 Application Notebook, Vol 30 No s2, in an interactive PDF format.

The new Agilent 1260 Infinity Hybrid SFC/UHPLC System packs two orthogonal separation modes into one instrument, bringing you more information from a single automated sequence.

Merck Millipore has announced that it has been invited to serve on the faculty of the Centre for Pharmaceutical Information and Engineering Research (CPIER) at Peking University, China.

Shimadzu has introduced the Nexera MP UHPLC as a Front End system for LC/MS. The Nexera MP is perfect for LC/MS analysis conducted in pharmacokinetics and synthesis stages in drug detection processes.

Agilent has announced that it has listed its Infinity Series 1200 liquid chromatography systems and 6000 Series mass spectrometry systems as Class I medical devices with the US Food and Drug Administration.

Thermo Scientific SOLA products revolutionize Solid Phase Extraction (SPE).

AB Sciex and Indigo BioSystems have announced an agreement to jointly market mass spectrometry solutions that streamline data acquisition and automate data review to ensure high quality results in clinical research, forensic toxicology and pre-clinical and clinical trials of new drugs.

Life Technologies Corporation has announced that they have signed an agreement with DaAn Gene, China?s premier bio-tech enterprise, to form Life Technologies DaAn Diagnostics.

Sample preparation is the basis for all separations-related research.

Agilent has announced that the National Centre for Genome Resources (NCGR) in Santa Fe, New Mexico, has achieved Certified Service Provider status for the Agilent SureSelect Target Enrichment System.

The 36th International Symposium on Capillary Chromatography (ISCC) 2012 has released the deadline dates for any abstracts for the symposium.

At a ceremony that coincided with the 20th anniversary of Los Angeles Laker Marvin ?Magic? Johnson?s public revelation that he had acquired Human Immunodeficiency Virus (HIV), the University at Buffalo?s School of Pharmacy and Pharmaceutical Sciences (Buffalo, New York) acknowledged Waters Corporation (Milford, Massachusetts) for its donation of an Acquity TQD System, a liquid chromatograph?mass spectrometer that will be used to build laboratory capacity and advance research into the treatment of HIV and Acquired Immune Deficiency Syndrome (AIDS)-related illnesses in sub-Saharan Africa.

Thermo EU - Demonstrating High-Performance Quantitative Analysis of Benzodiazepines using Multiplexed SIM with High-Resolution, Accurate Mass Detection on the Q Exactive LC/MS

Experimental Considerations

Supercritical fluid chromatography (SFC) is a quasi-gas phase technique used to separate a variety of compounds in natural products, fragrances, fine chemicals and pharmaceutical applications.

The cloning of animals by somatic cell nuclear transfer has been carried out successfully for many years, however, the survival rates of cloned animals is very low. This has been attributed to abnormal gene expression in cloned placentas that results in the loss of the foetus or the death of newly born animals.

Caffeine levels in espresso coffees purchased from coffee shops have been found to vary greatly and at well above the recommended daily allowance set by the Food Standards Agency.