CEM Corporation

Articles by CEM Corporation

More and more regulations regarding PFAS are being implemented with action limits that continue to decrease. Having a harmonized method to accurately determine the PFAS content in food, as well as other matrices, is important to ensuring long-term detection and regulation. The solvent extraction of PFAS from these varied sample matrices can be challenging given the susceptibility to contamination and the low levels in which these compounds are present. This poster, presented at RAFA 2024, examines the PFAS extraction several different food samples as well as food packing matrices.

PFAS have been shown to cause health issues in humans, which means monitoring environmental solid samples, such as soil and tissue, is critical. This application note details the extraction of 40 spiked PFAS compounds from soil and tissue following EPA Method 1633. The automated extraction was less than 10 minutes per sample and yielded acceptable recoveries and RSDs without carryover in the system. The EDGE PFAS is an ideal option for laboratories that want to automate their PFAS extractions of solid samples.

Existing solvent extraction techniques are predominantly manual methods that are not rapid, simple, or efficient. The EDGE PFAS™, an automated solvent extraction system, provides an automated, sequential approach to PFAS extraction. This system performs an efficient extraction of PFAS compounds from challenging food and food packaging matrices in one simple process. Upon completion, the final extract is filtered and ready for any minimal cleanup required, as well as analysis. Excellent recovery with tight reproducibility has been found. The EDGE PFAS method offers a rapid, simple, and efficient solvent extraction solution for PFAS testing.

Advances in Food Analysis: A Virtual Symposium

Webinar Dates/Times: Tuesday December 6th, 2022 Morning session: 1:00pm GMT -3:30pm GMT Afternoon session: 3:30pm GMT- 4:00pm GMT Wednesday, December 7th, 2022 Morning session: 1:00pm GMT -3:00pm GMT Afternoon session: 3:30pm GMT- 4:00pm GMT

Pesticide testing is crucial to assessing the safety of fruits and vegetables for consumption. The traditional extraction method for pesticides from produce is the QuEChERS method. This method is tedious, manual, time consuming, and wasteful. Thus, there is a need for improved methods of extraction. In this application note, the EDGE®, in combination with Q-Matrix™ Hydra, a water-removing sorbent, was used to extract a panel of pesticides from 10 g of homogenized cucumber, tomato, and green pepper in less than 9 min. The recoveries of the pesticide panel were greater than 70% for each matrix tested, and these results were highly reproducible. The EDGE provides a fully automated extraction that combines both the sample and sorbent into one sample vessel, alleviating the human burden of extraction and the need for multiple sample transfers.

In order to evaluate and test the robustness of cannabinoid analysis using the miniLC, a method was chosen from the literature and compared to data from the miniLC system. Comparison of retention time of standards to published values indicates the miniLC provides an excellent alternative with comparable results to a more expensive, complicated liquid chromatography system

Monday, July 19, 2021, 02:00 PM EDT Tuesday, July 20, 2021, 02:00 PM EDT Join us for this free online event to learn about important developments in the analysis of contaminants in a wide range of food and environmental matrices using a range of chromatographic, detection, and sample preparation techniques. A few hours of your time will deliver enormous benefits for your work.

ChromTalks: The Benefit of Hindsight in Chromatography

***Thursday and Friday May 13-14 | May 20-21, 2021*** In the relaxed and unconventional talks in this symposium, highly experienced speakers from industry and academia will impart key learnings from their long experience with chromatography—from heroic failures that have taught them valuable lessons, to moments of inspirational serendipity, and everything in between. CHROMTalks will deliver lifetimes of learning in condensed form, covering topics across implementation, troubleshooting, and method development of analytical techniques. Time spent at CHROMTalks will pay back as soon as you enter your laboratory! ***Available On Demand Until May 21, 2022***

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